Skip to main content
Log in

Additive manufacturing of nickel-based superalloy Inconel 718 by selective electron beam melting: Processing window and microstructure

  • Metal
  • Article
  • Published:
Journal of Materials Research Aims and scope Submit manuscript

Abstract

Cube-shaped IN718 samples were produced by selective electron beam melting (SEBM) with varying beam power, deflection speed, and beam spot size. Process parameter windows were identified where fully dense samples are obtained with no surface unevenness. High deflection speeds were demonstrated to result in smaller demand of area energy. This result is explained by the reduced time for heat dissipation into the substrate during hatching. The grain structure was strongly affected by SEBM process parameters. Under certain conditions, epitaxial growth over many layers and well-developed columnar grain structures were obtained with a polycrystalline substrate plate. A more defocused beam led to a lower melt pool temperature and shallower melt pool geometry where maximum temperature gradients and solidification rates were more or less in parallel with the building direction and primary dendrite arm orientation. These conditions help to suppress grain nucleation ahead of the nucleation front as vigorous melt movement, fragmentation of dendrites, and tertiary arm growth are suppressed.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

FIG. 1
FIG. 2
FIG. 3
FIG. 4
FIG. 5
FIG. 6
FIG. 7
FIG. 8
FIG. 9
FIG. 10
FIG. 11
FIG. 12
FIG. 13

Similar content being viewed by others

References

  1. N. Hopkinson, R. Hague, and P. Dickens: Rapid Manufacturing: An Industrial Revolution for the Digital Age, 1st ed. (Wiley, Camberley, England, 2006).

    Google Scholar 

  2. P. Blackwell: The mechanical and microstructural characteristics of laser-deposited IN718. J. Mater. Process. Technol. 170(1–2), 240 (2005).

    Article  CAS  Google Scholar 

  3. A. Strondl, R. Fischer, G. Frommeyer, and A. Schneider: Investigations of MX and γ′/γ″ precipitates in the nickel-based superalloy 718 produced by electron beam melting. Mater. Sci. Eng., A 480(1–2), 138 (2008).

    Article  Google Scholar 

  4. A. Strondl, M. Palm, J. Gnauk, and G. Frommeyer: Microstructure and mechanical properties of nickel based superalloy IN718 produced by rapid prototyping with electron beam melting (EBM). Mater. Sci. Technol. 27(5), 876 (2009).

    Article  Google Scholar 

  5. A. Strondl, S. Milenkovic, A. Schneider, U. Klement, and G. Frommeyer: Effect of processing on microstructure and physical properties of three nickel-based superalloys with different hardening mechanisms. Adv. Eng. Mater. 14(7), 427 (2012).

    Article  CAS  Google Scholar 

  6. K.N. Amato, S.M. Gaytan, L.E. Murr, E. Martinez, P.W. Shindo, J. Hernandez, S. Collins, and F.R. Medina: Microstructures and mechanical behavior of Inconel 718 fabricated by selective laser melting. Acta Mater. 60(5), 2229 (2012).

    Article  CAS  Google Scholar 

  7. Z. Wang, K. Guan, M. Gao, X. Li, X. Chen, and X. Zeng: The microstructure and mechanical properties of deposited-IN718 by selective laser melting. J. Alloys Compd. 513(0), 518 (2012).

    Article  CAS  Google Scholar 

  8. P. Heinl, L. Müller, C. Körner, R.F. Singer, and F.A. Müller: Cellular Ti–6Al–4V structures with interconnected macro porosity for bone implants fabricated by selective electron beam melting. Acta Biomater. 4(5), 1536 (2008).

    Article  CAS  Google Scholar 

  9. X. Zhao, J. Chen, X. Lin, and W. Huang: Study on microstructure and mechanical properties of laser rapid forming Inconel 718. Mater. Sci. Eng., A 478(1–2), 119 (2008).

    Article  Google Scholar 

  10. H. Qi, M. Azer, and A. Ritter: Studies of standard heat treatment effects on microstructure and mechanical properties of laser net shape manufactured INCONEL 718. Metall. Mater. Trans. A 40(10), 2410–2422 (2009).

    Article  Google Scholar 

  11. A. Klassen, T. Scharowsky, and C. Körner: Evaporation model for beam based additive manufacturing using free surface lattice Boltzmann methods. J. Phys. D: Appl. Phys. 47(27), 275 (2014).

    Article  Google Scholar 

  12. H.S. Carslaw and J.C. Jaeger: Conduction of Heat in Solids, 2nd ed. (Oxford University Press, New York, 1959), pp. 58–62.

    Google Scholar 

  13. G. Pottlacher, H. Hosaeus, E. Kaschnitz, and A. Seifter: Thermophysical properties of solid and liquid Inconel 718 alloy. Scand. J. Metall. 31(3), 161 (2002).

    Article  CAS  Google Scholar 

  14. R. Ito, P. Andreo, and T. Tabata: Reflection ratios of electrons and photons from solids. Bull. Univ. Osaka Prefect., Ser. A 41(2), 69 (1992).

    CAS  Google Scholar 

  15. T. Tabata, P. Andreo, and K. Shinoda: Fractional energies of backscattered electrons and photon yields by electrons. Radiat. Phys. Chem. 54(1), 11 (1999).

    Article  CAS  Google Scholar 

  16. D. Walton and B. Chalmers: The origin of the preferred orientation in the columnar zone of ingots. Trans. Metall. Soc. AIME 215(6), 1 (1959).

    Google Scholar 

  17. M. Gäumann, C. Bezençon, P. Canalis, and W. Kurz: Single-crystal laser deposition of superalloys: Processing–microstructure maps. Acta Mater. 49(6), 1051 (2001).

    Article  Google Scholar 

  18. L. Thijs, F. Verhaeghe, T. Craeghs, J.V. Humbeeck, and J.P. Kruth: A study of the microstructural evolution during selective laser melting of Ti-6Al-4V. Acta Mater. 58(9), 3303 (2010).

    Article  CAS  Google Scholar 

  19. M. Gäumann, S. Henry, F. Cléton, J-D. Wagnière, and W. Kurz: Epitaxial laser metal forming: Analysis of microstructure formation. Mater. Sci. Eng., A 271(1–2), 232 (1999).

    Article  Google Scholar 

  20. R. Trivedi and W. Kurz: Dendritic growth. Int. Mater. Rev. 39(2), 49 (1994).

    Article  CAS  Google Scholar 

  21. M. Rappaz, S.A. David, J.M. Vitek, and L.A. Boatner: Development of microstructures in Fe−15Ni−15Cr single crystal electron beam welds. Metall. Mater. Trans. A 20(6), 1125 (1989).

    Article  Google Scholar 

  22. M. Rappaz, S.A. David, J.M. Vitek, and L.A. Boatner: Analysis of solidification microstructures in Fe-Ni-Cr single-crystal welds. Metall. Mater. Trans. A 21(6), 1767 (1990).

    Article  Google Scholar 

  23. S. Mokadem, C. Bezençon, A. Hauert, A. Jacot, and W. Kurz: Laser repair of superalloy single crystals with varying substrate orientations. Metall. Mater. Trans. A 38(7), 1500 (2007).

    Article  Google Scholar 

Download references

ACKNOWLEDGMENTS

The authors gratefully acknowledge funding by the Deutsche Forschungsgemeinschaft (DFG) through the Collaborative Research Center SFB/Transregio 103, Project B2.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Harald Ernst Helmer.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Helmer, H.E., Körner, C. & Singer, R.F. Additive manufacturing of nickel-based superalloy Inconel 718 by selective electron beam melting: Processing window and microstructure. Journal of Materials Research 29, 1987–1996 (2014). https://doi.org/10.1557/jmr.2014.192

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1557/jmr.2014.192

Navigation