Abstract
The use of three-dimensional x-ray structural microscopy for nondestructive investigations of the deformation microstructure under microindents was demonstrated. Point to point, micrometer-resolution x-ray microbeam measurements of local lattice rotations were made for selected positions under 100-mN Berkovich and conical indents in single-crystal copper. Local lattice orientation measurements were used to extract micrometer by micrometer lattice misorientations and rotation axes along x-ray microbeams. Measurements of the deformation microstructure in symmetry and off-symmetry geometries are reported and discussed in terms of their potential for fundamental deformation investigations.
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Y. Huang, Z. Xue, H. Gao, W.D. Nix, and Z.C. Xia, J. Mater. Res. 15, 1786 (2000).
C.F. Robertson and M.C. Fivel, J. Mater. Res. 14, 2251 (1999).
J.G. Swadener, E.P. George, and G.M. Pharr, J. Mech. Phys. Solids 50, 681 (2002).
Z. Xue, Y. Huang, K.C. Hwang, and M. Li, J. Eng. Mater–T ASME, 124, 371 (2002).
W.D. Nix and H. Gao, J. Mech. Phys. Solids 46, 411, (1998).
N.A. Fleck and J.W. Hutchinson, Adv. Appl. Mech. 33, 295 (1997).
Q. Ma and D.R. Clarke, J. Mater. Res. 10, 853 (1995).
J.E. Bradby, J.S. Williams, J. Wong-Leung, M.V. Swain, and P. Munroe, Appl. Phys. Lett. 77, 3749 (2000).
W. Zielinski, H. Huang, and W.W. Gerberich, J. Mater. Res. 8, 1300 (1993).
S. Harvey, H. Huang, S. Venkataraman, and W.W. Gerberich, J. Mater. Res. 8, 1291 (1993).
D.F. Bahr, K.A. Nibur, K.R. Morasch, and D.P. Field, JOM 55, 47 (2003).
L.N. Brewer, M.A. Othon, L.M. Young, and T.M. Angeliu, Microsc. Microanal. 8, 684CD (2002).
D.A. Hughes, N. Hansen, and D.J. Bammann, Scr. Mater. 48, 147 (2003).
L. Margulies, G. Winther, and H.F. Poulsen, Science 192, 2392 (2001).
H.F. Poulsen and D. Juul Jensen, Mater. Sci. Forum 408–412, 49 (2002).
H.F. Poulsen and S. Schmidt, J. Appl. Cryst. 36, 319 (2003).
B.C. Larson, W. Yang, G.E. Ice, J.D. Budai, and J.Z. Tischler, Nature 415, 887 (2002).
G.E. Ice and B.C. Larson, Adv. Eng. Mater. 2, 643 (2000).
W. Yang, B.C. Larson, G.E. Ice, J.Z. Tischler, J.D. Budai, K-S. Chung, and W.P. Lowe, Appl. Phys. Lett. 82, 3856 (2003).
B.C. Larson, W. Yang, J.Z. Tischler, G.E. Ice, J.D. Budai, W. Liu, and H. Weiland, Int. J. Plast. 20, 543 (2004).
J-S. Chung and G.E. Ice, J. Appl. Phys. 86, 5249 (1999).
W. Yang, B.C. Larson, G.M. Pharr, G.E. Ice, J.G. Swadener, J.D. Budai, J.Z. Tischler, and W. Liu, in Surface Engineering 2002—Synthesis, Characterization and Applications, edited by A. Kumar, W.J. Meng, Y-T. Cheng, J.S. Zabinski, G.L. Doll, and S. Veprek (Mater. Res. Soc. Symp. Proc. 750, Warrendale, PA, 2003), pp. 115–118.
W. Yang, B.C. Larson, G.M. Pharr, G.E. Ice, J.Z. Tischler, J.D. Budai, and W. Liu, in Multiscale Phenomena in Materials— Experiments and Modeling Related to Mechanical Behavior, edited by H.M. Zbib, D.H. Lassila, L.E. Levine, and K.J. Hemker (Mater. Res. Soc. Symp. Proc. 779, Warrendale, PA, 2003), pp. 207–212.
R. Barabash, G.E. Ice, B.C. Larson, G.M. Pharr, K-S. Chung, and W. Yang, Appl. Phys. Lett. 79, 4 (2001).
H. Gao, Y. Huang, and W.D. Nix, Naturwissenschaften 86, 507 (1999).
J.A. Knapp, D.M. Follstaedt, S.M. Myers, J.C. Barbour, and T.A. Friedman, J. Appl. Phys 85, 1460 (1999).
M.C. Fivel, C.F. Robertson, G.R. Canova, and L. Boulanger, Acta Mater 46, 6183 (1998).
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Yang, W., Larson, B.C., Pharr, G.M. et al. Deformation microstructure under microindents in single-crystal Cu using three-dimensional x-ray structural microscopy. Journal of Materials Research 19, 66–72 (2004). https://doi.org/10.1557/jmr.2004.19.1.66
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DOI: https://doi.org/10.1557/jmr.2004.19.1.66