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Large-quantity production of high-yield boron nitride nanotubes

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Abstract

A high quantity and yield (up to 85%) of boron nitride (BN) nanotubes have been produced using a mechanothermal method. Elemental boron powders were first mechanically milled at room temperature in NH3 atmosphere and subsequently heated in N2 gas at 1200 °C for up to 16 h. The BN nanotubes obtained have either multiwalled cylindrical or bamboolike structures, suggesting different growth processes. The high formation yield of BN nanotubes is due to a high density of nanostructured nuclei created by an extensive milling treatment.

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References

  1. N.G. Chopra, R.J. Luyken, K. Cherrey, V.H. Crespi, M.L. Cohen, S.G. Louie, and A. Zettl, Science 269, 966 (1995).

    Article  CAS  Google Scholar 

  2. A. Loiseau, F. Williame, N. Demoncy, G. Hug, and H. Pascard, Phys. Rev. Lett. 76, 4737 (1996).

    Article  CAS  Google Scholar 

  3. M. Terrones, W.K. Hsu, H. Terrones, J.P. Zhang, S. Ramos, J.P. Hare, R. Castillo, K. Prassides, A.K. Cheetham, H.K. Kroto, and D.R.M. Walton, Chem. Phys. Lett. 259, 568 (1996).

    Article  CAS  Google Scholar 

  4. D. Golberg, Y. Bando, M. Eremets, K. Takemura, K. Kurashima, and H. Yusa, Appl. Phys. Lett. 69, 2045 (1996).

    Article  CAS  Google Scholar 

  5. T. Laude, Y. Matsui, A. Marraud, and B. Jouffrey, Appl. Phys. Lett. 76, 3239 (2000).

    Article  CAS  Google Scholar 

  6. P. Gleize, M.C. Schouler, P. Gadelle, and M. Caillet, J. Mater. Sci. 29, 1575 (1994).

    Article  CAS  Google Scholar 

  7. T.S. Bartnitskaya, G.S. Oleinik, A.V. Pokropivnyi, and V.V. Pokropivnyi, JETP Lett. 69, 163 (1999).

    Article  CAS  Google Scholar 

  8. O.R. Lourie, C.R. Jones, B.M. Bartlett, P.C. Gibbons, R.S. Ruoff, and W.E. Buhro, Chem. Mater. 12, 1808 (2000).

    Article  CAS  Google Scholar 

  9. P. Ma, Y. Bando, and T. Sato, Chem. Phys. Lett. 337, 61 (2001).

    Article  CAS  Google Scholar 

  10. W. Han, Y. Bando, K. Kurashima, and T. Sato, Appl. Phys. Lett. 73, 3085 (1998).

    Article  CAS  Google Scholar 

  11. J. Cumings and A. Zettl, Chem. Phys. Lett. 316, 211 (2000).

    Article  CAS  Google Scholar 

  12. R.S. Lee, J. Gavillet, M. Lamy de la Chapelle, A. Loiseau, J-L. Cochon, D. Pigache, J. Thibault, and F. Williame, Phys. Rev. B 64, 121405 (2001).

    Article  Google Scholar 

  13. Y. Chen, J. Fitz Gerald, J.S. Williams, and S. Bulcock, Chem. Phys. Lett. 299, 260 (1999).

    Article  CAS  Google Scholar 

  14. Y. Chen, J. Fitz Gerald, J.S. Williams, and P. Willis, Mater. Sci. Forum 312, 173 (1999).

    Article  Google Scholar 

  15. Y. Chen, T. Halstead, and J.S. Williams, Mater. Sci. Eng. A 206, 24 (1996).

    Article  Google Scholar 

  16. Y. Chen and J. Fitzgerald (unpublished results).

  17. L.T. Chadderton and Y. Chen, Phys. Lett. A 263, 401 (1999).

    Article  CAS  Google Scholar 

  18. Y. Chen, L.T. Chadderton, J.S. Williams, and J. Fitz Gerald, Mater. Sci. Forum 343, 63 (2000).

    Article  Google Scholar 

  19. Y. Chen, L.T. Chadderton, J. Fitz Gerald, and J.S. Williams, Appl. Phys. Lett. 74, 2960 (1999).

    Article  CAS  Google Scholar 

  20. S.R. Logan and C. Kemball, Trans. Faraday Soc. 57, 44 (1959).

    Google Scholar 

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Chen, Y., Conway, M., Williams, J.S. et al. Large-quantity production of high-yield boron nitride nanotubes. Journal of Materials Research 17, 1896–1899 (2002). https://doi.org/10.1557/JMR.2002.0281

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  • DOI: https://doi.org/10.1557/JMR.2002.0281

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