Hostname: page-component-76fb5796d-45l2p Total loading time: 0 Render date: 2024-04-25T09:06:52.672Z Has data issue: false hasContentIssue false

Indentation-induced two-way shape-memory effect in aged Ti-50.9 at.% Ni

Published online by Cambridge University Press:  02 January 2015

Mareike Frensemeier*
Affiliation:
INM—Leibniz Institute for New Materials, Saarbrücken 66123, Germany; Saarland University, Saarbrücken 66123, Germany
Eduard Arzt
Affiliation:
INM—Leibniz Institute for New Materials, Saarbrücken 66123, Germany; Saarland University, Saarbrücken 66123, Germany
Enwei Qin
Affiliation:
Suzhou Nuclear Power Research Institute Co., Ltd., Suzhou 215004, China
Carl P. Frick
Affiliation:
Department of Mechanical Engineering, University of Wyoming, Laramie, Wyoming 82071
Andreas S. Schneider
Affiliation:
INM—Leibniz Institute for New Materials, Saarbrücken 66123, Germany
*
Address all correspondence to Mareike Frensemeier atmareike.frensemeier@inm-gmbh.de
Get access

Abstract

In this study, Vickers indentation was used to investigate the two-way shape-memory effect (TWSME) in an austenitic Ti-50.9 at.% Ni alloy, exposed to different heat treatments. Three aging treatments were used to manipulate the size of Ti3Ni4 precipitates. All samples were Vickers indented, and the indent depth was investigated as function of thermal cycling. The TWSME was found only in the material aged at 400 °C, which contained coherent precipitates. Thermal cycling shows stable TWSME, however, heating well above the austenite finish temperature lead to permanent austenitic protrusions. The results indicate that stabilized martensite plays a critical role in creating TWSME surfaces.

Type
Research Letters
Copyright
Copyright © Materials Research Society 2015 

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

1.Shaw, J.A. and Kyriakides, S.: Thermomechanical aspects of NiTi. J. Mech. Phys. Solids 43, 12431281 (1995).Google Scholar
2.Otsuka, K. and Ren, X.: Physical metallurgy of Ti-Ni-based shape memory alloys. Prog. Mater. Sci. 50, 511678 (2005).Google Scholar
3.Zhang, Y.J., Cheng, Y.T., and Grummon, D.S.: Shape memory surfaces. Appl. Phys. Lett. 89, 041912 (2006).Google Scholar
4.Zhang, Y.J., Cheng, Y.T., and Grummon, D.S.: Understanding indentation-induced two-way shape memory effect. J. Mater. Res. 22, 28512855 (2007).Google Scholar
5.Fei, X.L., Zhang, Y.J., Grummon, D.S., and Cheng, Y.T.: Indentation-induced two-way shape memory surfaces. J. Mater. Res. 24, 823830 (2009).Google Scholar
6.Qin, E., Peter, N.J., Frensemeier, M., Frick, C.P., Arzt, E., and Schneider, A.S.: Vickers indentation induced one-way and two-way shape memory effect in austenitic NiTi. Adv. Eng. Mater. 16, 7279 (2014).CrossRefGoogle Scholar
7.Gall, K., Sehitoglu, H., Chumlyakov, Y.I., Kireeva, I.V., and Maier, H.J.: The influence of aging on critical transformation stress levels and martensite start temperatures in NiTi: part II—discussion of experimental results. J. Eng. Mater. 121, 2837 (1999).Google Scholar
8.Gall, K., Sehitoglu, H., Chumlyakov, Y.I., Kireeva, I.V., and Maier, H.J.: The influence of aging on critical transformation stress levels and martensite start temperatures in NiTi: part I—aged microstructure and micro-mechanical modeling. J. Eng. Mater. 121, 1927 (1999).Google Scholar
9.Liu, Y.N., Yang, H., and Voigt, A.: Thermal analysis of the effect of aging on the transformation behaviour of Ti-50.9 at. % Ni. Mater. Sci. Eng. A 360, 350355 (2003).CrossRefGoogle Scholar
10.Khalil-Allafi, J., Dlouhy, A., and Eggeler, G.: Ni4Ti3-precipitation during aging of NiTi shape memory alloys and its influence on martensitic phase transformations. Acta Mater. 50, 42554274 (2002).CrossRefGoogle Scholar
11.Frick, C.P., Ortega, A.M., Tyber, J., Maksound, A.E.M., Maier, H.J., Liu, Y.N., and Gall, K.: Thermal processing of polycrystalline NiTi shape memory alloys. Mater. Sci. Eng. A 405, 3449 (2005).Google Scholar
12.Ni, W.Y., Cheng, Y.T., and Grummon, D.S.: Recovery of microindents in a nickel–titanium shape-memory alloy: a “self-healing” effect. Appl. Phys. Lett. 80, 33103312 (2002).Google Scholar
13.Shaw, G.A., Stone, D.S., Johnson, A.D., Ellis, A.B., and Crone, W.C.: Shape memory effect in nanoindentation of nickel–titanium thin films. Appl. Phys. Lett. 83, 257259 (2003).Google Scholar
14.Otsuka, K. and Wayman, C.M.: Shape Memory Materials (Cambridge University Press, Cambridge, UK, 1998).Google Scholar
15.Lin, H.C., Wu, S.K., Chou, T.S., and Kao, H.P.: The effects of cold-rolling on the martensitic-transformation of an equiatomic tini alloy. Acta Metall. Mater. 39, 20692080 (1991).Google Scholar
16.Liu, Y.N. and Favier, D.: Stabilisation of martensite due to shear deformation via variant reorientation in polycrystalline NiTi. Acta Mater. 48, 34893499 (2000).Google Scholar
17.Mahmud, A.S., Yang, H., Tee, S., Rio, G., and Liu, Y.: Effect of annealing on deformation-induced martensite stabilisation of NiTi. Intermetallics 16, 209214 (2008).CrossRefGoogle Scholar
18.Laplanche, G., Pfetzing-Micklich, J., and Eggeler, G.: Orientation dependence of stress-induced martensite formation during nanoindentation in NiTi shape memory alloys. Acta Mater. 68, 1931 (2014).Google Scholar
19.Pfetzing, J., Schaefer, A., Somsen, C., and Wagner, M.F.-X.: Nanoindentation of pseudoelastic NiTi shape memory alloys: thermomechanical and microstructural aspects. Int. J. Mater. Res. 100, 936942 (2009).CrossRefGoogle Scholar
20.Ye, C. and Cheng, G.J.: Scalable patterning on shape memory alloy by laser shock assisted direct imprinting. Appl. Surf. Sci. 258, 1004210046 (2012).CrossRefGoogle Scholar