Hostname: page-component-8448b6f56d-xtgtn Total loading time: 0 Render date: 2024-04-18T20:10:42.838Z Has data issue: false hasContentIssue false

Application of Dynamic Impedance Spectroscopy to Scanning Probe Microscopy

Published online by Cambridge University Press:  13 February 2014

Mateusz Tomasz Tobiszewski*
Affiliation:
Department of Electrochemistry, Corrosion and Materials Engineering, Gdańsk University of Technology, Narutowicza 11/12, 80-233 Gdańsk, Poland
Anna Arutunow
Affiliation:
Department of Electrochemistry, Corrosion and Materials Engineering, Gdańsk University of Technology, Narutowicza 11/12, 80-233 Gdańsk, Poland
Kazimierz Darowicki
Affiliation:
Department of Electrochemistry, Corrosion and Materials Engineering, Gdańsk University of Technology, Narutowicza 11/12, 80-233 Gdańsk, Poland
*
*Corresponding author. mateusztobiszewski@gmail.com
Get access

Abstract

Dynamic impedance spectroscopy, designed for measuring nonstationary systems, was used in combination with scanning probe microscopy. Using this approach, impedance mapping could be carried-out simultaneously with topography scanning. Therefore, correlation of electrical properties with particular phases of an examined sample was possible. The sample used in this study was spheroidal graphite cast iron with clearly defined phases having significantly different properties. Additionally, impedance-force curves were made at graphite precipitation and ferrite matrix to illustrate the relation between impedance and the force applied to a probe.

Type
Materials Applications
Copyright
© Microscopy Society of America 2014 

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Arutunow, A., Darowicki, K. & Tobiszewski, M.T. (2013 a). Electrical mapping of AISI 304 stainless steel subjected to intergranular corrosion performed by means of AFM–LIS in the contact mode. Corrosion Sci 71, 3742.Google Scholar
Arutunow, A., Darowicki, K. & Zieliński, A. (2011). Atomic force microscopy based approach to local impedance measurements of grain interiors and grain boundaries of sensitized AISI 304 stainless steel. Electrochim Acta 56, 23722377.CrossRefGoogle Scholar
Arutunow, A., Zieliński, A. & Tobiszewski, M.T. (2013 b). Localized impedance measurements of AA2024 and AA2024-T3 performed by means of AFM in contact mode. Anti-Corros Methods Mater 60, 6772.Google Scholar
Birbilis, N., Meyer, K., Muddle, B.C. & Lynch, S.P. (2009). In situ measurement of corrosion on the nanoscale. Corrosion Sci 51, 15691572.Google Scholar
Darowicki, K. (2000). Theoretical description of the measuring method of instantaneous impedance spectra. J Electroanal Chem 486, 101105.Google Scholar
Darowicki, K., Orlikowski, J. & Lentka, G. (2000). Instantaneous impedance spectra of a non-stationary model electrical system. J Electroanal Chem 486, 106110.CrossRefGoogle Scholar
Darowicki, K. & Ślepski, P. (2003). Dynamic electrochemical impedance spectroscopy of the first order electrode reaction. J Electroanal Chem 547, 18.CrossRefGoogle Scholar
Darowicki, K. & Ślepski, P. (2004). Instantaneous electrochemical impedance spectroscopy of electrode reactions. Electrochim Acta 49, 763772.Google Scholar
Darowicki, K., Zieliński, A. & Kurzydłowski, K.J. (2008). Application of dynamic impedance spectroscopy to atomic force microscopy. Sci Technol Adv Mater 9, 045006.Google Scholar
Galicia, G., Pébčre, N., Tribollet, B. & Vivier, V. (2009). Local and global electrochemical impedances applied to the corrosion behaviour of an AZ91 magnesium alloy. Corrosion Sci 51, 17891794.Google Scholar
Huang, V.M., Wu, S.L., Orazem, M.E., Pébčre, N., Tribollet, B. & Vivier, V. (2011). Local electrochemical impedance spectroscopy: A review and some recent developments. Electrochim Acta 56, 80488057.Google Scholar
Kalinin, S.V. & Bonnell, D.A. (2001). Scanning impedance microscopy of electroactive interfaces. Appl Phys Lett 78, 13061308.Google Scholar
Kalinin, S.V. & Bonnell, D.A. (2002). Scanning impedance microscopy of an active Schottky barrier diode. J Appl Phys 91, 832839.Google Scholar
Layson, A., Gadad, S. & Teeters, D. (2003). Resistance measurements at the nanoscale: Scanning probe AC impedance spectroscopy. Electrochim Acta 48, 22072213.Google Scholar
Layson, A.R. & Teeters, D. (2004). Polymer electrolytes confined in nanopores: Using water as a means to explore the interfacial impedance at the nanoscale. Solid State Ion 175, 773780.Google Scholar
Lohrengel, M.M., Heiroth, S., Kluger, K., Pilaski, M. & Walther, B. (2006). Microimpedance—Localized material analysis. Electrochim Acta 51, 14311436.Google Scholar
O’Hayre, R., Feng, G., Nix, W.D. & Prinz, F.B. (2004 a). Quantitative impedance measurement using atomic force microscopy. J Appl Phys 95, 35403549.Google Scholar
O’Hayre, R., Minhwan, L. & Prinz, F.B. (2004 b). Ionic and electronic impedance imaging using atomic force microscopy. J Appl Phys 95, 83828392.Google Scholar
Pingree, L.S.C. & Hersam, M.C. (2005). Bridge-enhanced nanoscale impedance microscopy. Appl Phys Lett 87, 233117.Google Scholar
Shao, R., Kalinin, S.V. & Bonnell, D.A. (2003). Local impedance imaging and spectroscopy of polycrystalline ZnO using contact atomic force microscopy. Appl Phys Lett 82, 18691871.Google Scholar
Tobiszewski, M.T., Zieliński, A. & Darowicki, K. (2013). Dynamic nanoimpedance characterization of the AFM tip-surface contact. Microsc Microanal. Published online 13 December 2013. Available at http://dx.doi.org/10.1017/S1431927613013895.Google Scholar