Journal of Materials Research

Articles

On the elastic moduli of nanocrystalline Fe, Cu, Ni, and Cu–Ni alloys prepared by mechanical milling/alloying

T.D. Shena1, C.C. Kocha1, T.Y. Tsuia2 and G.M. Pharra2

a1 Department of Materials Science and Engineering, North Carolina State University, Raleigh, North Carolina 27695-7907

a2 Department of Materials Science, Rice University, Houston Texas 77251-1892

Abstract

Young's moduli of nanocrystalline Fe, Cu, Ni, and Cu-Ni alloys prepared by mechanical milling/alloying have been measured by the nanoindentation technique. The results indicate that Young's moduli of nanocrystalline Cu, Ni, and Cu–Ni alloys with a grain size ranging from 17 to 26 nm are similar to those of the corresponding polycrystals. The dependence of Young's modulus of nanocrystalline Fe on grain size corresponds well to a theoretical prediction, which suggests that the change in the Young and shear moduli of nanocrystalline materials, free of porosity, with a grain size larger than about 4 nm, should be very limited (<10%). It is likely that reported large decreases in the Young and shear moduli of nanocrystalline materials prepared by gas-condensation/vacuum consolidation result from a relatively large volume fraction of pores.

(Received June 10 1995)

(Accepted August 04 1995)

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