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Powder diffraction data and Rietveld refinement of metastable t-ZrO2 at low temperature

Published online by Cambridge University Press:  10 January 2013

J. Málek ,
L. Beneš  and
T. Mitsuhashi
J. Málek
Affiliation:
Joint Laboratory of Solid State Chemistry, Academy of Sciences of the Czech Republic & University of Pardubice, Studenská 84, Pardubice 530 09, Czech Republic
L. Beneš*
Affiliation:
Joint Laboratory of Solid State Chemistry, Academy of Sciences of the Czech Republic & University of Pardubice, Studenská 84, Pardubice 530 09, Czech Republic
T. Mitsuhashi
Affiliation:
National Institute for Research in Inorganic Materials, 1-1 Namiki, Tsukuba, Ibaraki 305, Japan
*
a)Corresponding author.
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Abstract

Indexed X-ray powder diffraction data are reported for the low temperature tetragonal ZrO2 obtained by crystallization of zirconia gel. The structure was refined by the Rietveld technique on the basis of space group P42/nmc. Refined unit cell dimensions are a = 3.5984(5) Å, c = 5.152(1) Å, V = 66.71 Å3, Dx=6.135 g/cm3, F18=62 (0.012, 24), RP=8.99, Rwp=11.48, RB=3.13.

Type
Research Article
Information
Powder Diffraction , Volume 12 , Issue 2 , June 1997 , pp. 96 - 98
Copyright
Copyright © Cambridge University Press 1997

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